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`Searching PAJ
`
`1/1 Ail—‘3
`
`PATENT ABSTRACTS OF JAPAN
`
`(11)Publication number:
`
`2001-219496
`
`(43)Date of publication of application : 14.08.2001
`
`(51)Int.Cl.
`
`332B 9/00
`BOlJ 35/02
`B3213 17/10
`
`(21)Application number : 2000-363970
`
`(71)Applicant : TOTO LTD
`
`(22)Date of filing :
`
`30.11.2000
`
`(72)Inventor : MACHIDA MITSUYOSHI
`HAYAKAWA MAKOTO
`
`(30)Priority
`
`Priority number : 11341735
`
`Priority date : 01.12.1999
`
`Priority country : JP
`
`(54) FILM FOR WINDOW GLASS
`
`(57)Abstract:
`
`PROBLEM TO BE SOLVED: To provide a film for window glass not damaged in its light transmissivity and
`appearance even if used at an environmentally polluted place and having self-cleaning properties and easy
`cleaning properties.
`SOLUTION: In the film having self-cleaning properties for window glass constituted by forming a surface
`layer containing photocatalytic titanium oxide particles on a fiexibie base materiai, the surface aner
`generates no turbidity at a time of outdoor exposure, and the contact angle of the surface of the surface
`layer with water can become 20°
`or less corresponding to the irradiation of ultraviolet rays with a
`wavelength of 400 nm or less.
`
`http://www19.ipdl.inpit.go._jp/PA1/result/detail/main/wAAACGaunDA413219496P1htm
`
`2008/07/26
`
`

`

`JP,2001-219496,A [CLAIMS]
`
`>1: NOTICES =|<
`
`JPO and lNPlT are not responsible for any
`damages caused by the use of
`this translation.
`
`1/1 ’\°—°)
`
`1.This document has been translated by computer. So the translation may not reflect the original precisely.
`2.**** shows the word which can not be translated.
`
`3.In the drawings, any words are not translated.
`
`
`
`
`
`
`CLAIMS
`
`[Claim(s)]
`[Claim 1]On a substrate which has flexibility, a surface layer containing a hydrophilic component which is not
`the particle state which does not show light catalytic substantially by the exposure of a light catalytic
`titanium oxide particle and sunlight is formed, it is a film for windowpane attachment which has the self—
`cieaning nature from which an angle of contact with water will be 20 degrees or less according to an
`exposure of sunlight, Filter solution obtained by collecting affixes to said surface layer one month after an
`outdoor exposure, and a filtrate is extracted, A film for windowpane attachment, wherein sulfate ion (8042“)
`coating weight at the time of an outdoor exposure to said surface layer obtained by measuring this filtrate
`using a capillary eiectrophoresis device is below 750 ng/cmz.
`[Claim 2]Said light catalytic titanium oxide particle is an anatase type crystal or a brookite type crystal with a
`mean particle diameter of less than 40 nm, And the film for windowpane attachment according to claim 1,
`wherein the crystallite diameter is less than 6.0 nm and said light catalytic titanium oxide particle of said
`surface layer and composition ratio of said hydrophilic component are from 70 to 30 to 40 to 60 in a weight
`ratio.
`
`[Claim 3]The film for windowpane attachment according to claim 1 or 2, wherein specific surface area of the
`whole film using a surface area measuring instrument ("ASAP2010Ml' by Shimadzu) by a krypton (Kr) gas
`absorption method is below 0.150—m2/g.
`[Claim 4]The film for windowpane attachment according to claim 2 or 3, wherein said light catalytic titanium
`oxide particle is an anatase type crystal or a brookite type crystal with a mean particle diameter of 36 nm or
`less and the crystallite diameter is 5.5 nm or less.
`[Claim 5]The film for windowpane attachment according to claim 2 or 3, wherein said light catalytic titanium
`oxide particle is an anatase type crystal or a brookite type crystal with a mean particle diameter of 32 nm or
`less and the crystallite diameter is 5.0 nm or less.
`[Claim 6]The film for windowpane attachment according to claim 1 to 5, wherein at least a part of the
`hydrophilic components of said surface layer is silicone in which hydrophilization is carried out by
`photooatalysis at the time of an exposure of sunlight.
`[Claim 7]The film for windowpane attachment according to cfaim 1 to 6, wherein at least a part of the
`hydrophilic components of said surface layer is amorphous titanium oxide.
`[Claim 8]The film for windowpane attachment according to claim 1 to 7, wherein silica contains further in said
`surface layer.
`[Claim 9]The film for windowpane attachment according to claim 1 to 8, wherein said substrate is a high
`polymer resin film.
`[Claim 10]The film for windowpane attachment according to claim 9, wherein said poiymer resin is
`polyethylene terephthalate (PET), polycarbonate (PC), or polymethylmethacrylate (PMMA).
`
`[Translation done]
`
`http://www4.ipdl.lnpit.go,jp/cgi~bin/tran.,‘_web_cgiwejje?atw_u=http://www4.ipdl.inpit.go.jp/Tokujit... 2008/07/26
`
`

`

`
`
`
`
`
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`
`
`dP,2001-219496,A [DETAILED DESCRIPTION]
`
`1/10 ’Q—‘j
`
`* NOTICES *
`
`JPO and lNPlT are not responsible for any
`damages caused by the use of this translation.
`
`l.This document has been translated by computer. So the translation may not reflect the original precisely.
`2_**** shows the word which can not be translated.
`
`3.In the drawings, any words are not translated.
`
`DETAILED DESCRIPTION
`
`[Detailed Description of the Invention]
`[0001]
`[Field of the Invention]Even if air pollution, such as a big city, uses this invention at an intense place, it does
`not spoil translucency and appearance, and it relates to the film for windowpane attachment by which the dirt
`which adheres to the surface by a rainfall or backwashing by water is defe