Application No. 10/490,647
`
`Docket No.: HOK-0228
`
`AMENDMENTS TO THE CLAIMSa COMPLETE LISTING OF CLAIMS
`
`IN ASCENDING ORDER WITH STATUS INDICATOR
`
`Please amend the following claims as indicated.
`
`1. (Currently Amended) An antifouling film coated article having a film obtained by
`
`curing efia silicone resin material on a substrate, wherein a contact angle of water on said film is
`
`in a range of 5 to 30°, and an average surface roughness of said film is 5 nm or less.
`
`2. (Original) The antifouling film coated article as set forth in claim 1, wherein the
`
`contact angle of water on said film is in a range of 8 to 25°.
`
`3. (Currently Amended) The antifouling film coated article as set forth in claim 1,
`
`wherein the silicone resin material of said film is derived from a composition containing
`
`colloidal silica and a silicone resin that is at least one ofa partial hydrolysate and full
`
`hydrolysate of 4-functional hydrolyzable organosilane.
`
`4. (Original) The antifouling film coated article as set forth in claim 3, wherein said
`
`composition contains the colloidal silica such that a weight ratio of a solid content of silica to the
`
`solid content in terms of condensate of the silicone resin is in a range of 0.01 to 9.
`
`5. (Original) The antifouling film coated article as set forth in claim 3, wherein said
`
`composition further contains an organic zirconium.
`
`6. (Original) The antifouling film coated article as set forth in claim 5, wherein said
`
`composition contains 0.1 to 10 parts by weight of the organic zirconium in terms of Zr02 with
`
`respect to 100 parts by weight of the entire solid contents of said composition.
`
`7. (Original) The antifouling film coated article as set forth in claim 3, wherein said
`
`composition further contains an optical semiconductor material.
`
`
`
`Docket No.: HOK-0228
`
`AMENDMENTS TO THE CLAIMSa COMPLETE LISTING OF CLAIMS
`
`IN ASCENDING ORDER WITH STATUS INDICATOR
`
`Please amend the following claims as indicated.
`
`1. (Currently Amended) An antifouling film coated article having a film obtained by
`
`curing efia silicone resin material on a substrate, wherein a contact angle of water on said film is
`
`in a range of 5 to 30°, and an average surface roughness of said film is 5 nm or less.
`
`2. (Original) The antifouling film coated article as set forth in claim 1, wherein the
`
`contact angle of water on said film is in a range of 8 to 25°.
`
`3. (Currently Amended) The antifouling film coated article as set forth in claim 1,
`
`wherein the silicone resin material of said film is derived from a composition containing
`
`colloidal silica and a silicone resin that is at least one ofa partial hydrolysate and full
`
`hydrolysate of 4-functional hydrolyzable organosilane.
`
`4. (Original) The antifouling film coated article as set forth in claim 3, wherein said
`
`composition contains the colloidal silica such that a weight ratio of a solid content of silica to the
`
`solid content in terms of condensate of the silicone resin is in a range of 0.01 to 9.
`
`5. (Original) The antifouling film coated article as set forth in claim 3, wherein said
`
`composition further contains an organic zirconium.
`
`6. (Original) The antifouling film coated article as set forth in claim 5, wherein said
`
`composition contains 0.1 to 10 parts by weight of the organic zirconium in terms of Zr02 with
`
`respect to 100 parts by weight of the entire solid contents of said composition.
`
`7. (Original) The antifouling film coated article as set forth in claim 3, wherein said
`
`composition further contains an optical semiconductor material.
`
`
`
`Application No. 10/490,647
`
`Docket No.: PICK-0228
`
`8. (Original) The antifouling film coated article as set forth in claim 7, wherein a
`
`compounding ratio by weight of the optical semiconductor material to a total weight of the solid
`
`content in the terms of condensate of the silicone resin and silica as the solid content of the
`
`colloidal silica is 0.01 or more and less than 0.4.
`
`9. (Previously Presented) The antifouling film coated article as set forth in claim 3,
`
`wherein said composition contains an optical semiconductor material such that a compounding
`
`ratio by weight of the optical semiconductor material to the solid content in terms of condensate
`
`of the silicone resin is 0.01 or more and less than 0.4, and further contains 0.1 to 10 parts by
`
`weight of an organic zirconium in terms of ZrOz with respect to 100 parts by weight of the entire
`
`solid contents of said composition.
`
`10. (Original) The antifouling film coated article as set forth in claim 1, wherein said
`
`substrate is made of glass.
`
`1 1. (Previously Presented) The antifouling film coated article as set forth in claim 5,
`
`wherein said organic Zirconium comprises a compound shown in the following chemical
`
`formula
`
`Zr on R3m (OR1 )p
`
`(10)
`
`wherein (i) m and p are an integer ofO to 4, and n is 0 or 1, (ii) in the case of n=0, m+p=4, and
`
`(iii) in the case of n=1 , m+p=2.
`
`12. (Previously Presented) The antifouling film coated article as set forth in claim 11,
`
`wherein said organic zirconium is at least one selected from the group consisting of
`
`ZI‘(OC4H9)3 (C5H7Oz) and ZI'(OC4H9)2(C5H702)(C6H903).
`
`13. (Previously Presented) The antifouling film coated article as set forth in claim 1 1,
`
`wherein, in the chemical formula (10), (a) Rl is a monovalent hydrocarbon group, (b) R3
`
`comprises a C5H702 (acetylacetonate complex) or C6H903 (ethyl acetoacetate complex) and (c)
`
`different kinds of OR'and R3 may be included in one molecule.
`
`
`
`Application No. 10/490,647
`
`Docket No.2 HOK-0228
`
`14. (New) A method of forming an antifouling film coated article comprising the
`
`steps of:
`
`applying a silicone resin material on a substrate; and
`
`curing a resultant film on said substrate by a condensation polymerization reaction of
`
`said silicone resin material to obtain a cured film having a contact angle of water on said film in
`
`a range of 5 to 30°, and an average surface roughness of 5 nm or less.
`
`15. (New) The method as set forth in claim 14, wherein the silicone resin material of
`
`said film is a composition containing colloidal silica and a silicone resin that is at least one of a
`
`partial hydrolysate and full hydrolysate of 4-functional hydrolyzable organosilane.
`
`16. (New) The method as set forth in claim 14, wherein said composition further
`
`contains an organic zirconium.
`
`17. (New) The method as set forth in claim 16, wherein said organic zirconium
`
`comprises a compound shown in the following chemical formula
`
`Zr on R3,n (OR')p
`
`wherein (i) m and p are an integer of 0 to 4, “n” is 0 or 1, (ii) in the case of n=0, m+p=4, and (iii)
`
`in the case of n=1 , m+p=2.
`
`18. (New) The method as set forth in claim 17, wherein said organic zirconium is at
`
`least one selected from the group consisting of Zr(OC4H9)3(C5H702) and
`
`ZY(OC4H9)2(C5H702)(C6H903).
`
`19. (New) The method as set forth in claim 17, wherein, in the chemical formula
`
`(10), (a) R1 is a monovalent hydrocarbon group, (b) R3 comprises C5H702 (acetylacetonate
`
`complex) or C5H903 (ethyl acetoacetate complex) and (c) different kinds of OR1 and R3 may be
`
`included in one molecule.
`
`20. (New) The method as set forth in claim 15, wherein said composition contains the
`
`colloidal silica such that a weight ratio ofa solid content of silica to the solid content in terms of
`
`condensate ofthe silicone resin is in a range of 0.01 to 9.
`
`4
`
`
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